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KMID : 0380620110430030348
Korean Journal of Food Science and Technology
2011 Volume.43 No. 3 p.348 ~ p.360
Analysis of Off-flavor Compounds from Over-extracted Coffee
Lee Jin-sung

Kim Min-Sun
Shin Ho-Jae
Park Ki-Hwan
Abstract
To verify the volatile compounds contributing to coffee off-flavor, medium roasted Colombian, Sumatra, Ethiopian and light and dark roasted Colombian bean coffees were sequentially and studiously over extracted. Eight espresso samples and eight filter-dripped samples were analyzed by gas chromatography/mass spectrometry with the solidphase microextraction method and evaluated by sensory tests. In total, 67 compounds were detected, and desirable aroma decreased sharply, while off-flavors increased rapidly after 30 mL of espresso and 200 mL of drip coffee. Percent peak area of 4-ethylguaiacol revealed a linear increase during extraction and was highly correlated with increasing off-flavor, suggesting that it could be an indicator of over extraction. Considering the odor activity value, guaiacol and 4- vinylguaiacol were also contributory compounds to off-flavors.
KEYWORD
coffee, over-extraction, off-flavor, guaiacols, 4-ethylguaiacol
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